6U3N
LS2.8/3.15 - DQ2-P.fluor-alpha1a complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-02-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.94640 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 59.980, 239.470, 147.460 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.480 - 2.800 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.480 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rpim | 0.028 | 0.418 |
Number of reflections | 53350 | 5211 |
<I/σ(I)> | 17.05 | 1.85 |
Completeness [%] | 99.9 | 99.92 |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 22% PEG3350, 0.2M Na-K Tartrate, 0.1M MES pH6.5 |