6U3N

LS2.8/3.15 - DQ2-P.fluor-alpha1a complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX1
Synchrotron site	Australian Synchrotron
Beamline	MX1
Temperature [K]	100
Detector technology	CCD
Collection date	2017-02-10
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.94640
Spacegroup name	C 2 2 21
Unit cell lengths	59.980, 239.470, 147.460
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.480 - 2.800
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	46.480	2.900
High resolution limit [Å]	2.800	2.800
Rpim	0.028	0.418
Number of reflections	53350	5211
<I/σ(I)>	17.05	1.85
Completeness [%]	99.9	99.92
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	22% PEG3350, 0.2M Na-K Tartrate, 0.1M MES pH6.5