6TXK
Crystal structure of thermotoga maritima E65K Ferritin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.3 |
Synchrotron site | BESSY |
Beamline | 14.3 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-05-18 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.895 |
Spacegroup name | H 3 2 |
Unit cell lengths | 175.811, 175.811, 354.136 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.440 - 2.359 |
R-factor | 0.2019 |
Rwork | 0.201 |
R-free | 0.23650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1vlg |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.8.3) |
Refinement software | PHENIX (1.15.1_3469) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 20.440 | 20.440 | 2.500 |
High resolution limit [Å] | 2.359 | 7.010 | 2.360 |
Rmerge | 0.230 | 0.050 | 1.531 |
Rmeas | 0.248 | 0.055 | 1.645 |
Number of reflections | 86438 | 3414 | 13809 |
<I/σ(I)> | 8.72 | 28.04 | 1.33 |
Completeness [%] | 99.8 | 97.5 | 99.6 |
Redundancy | 7.516 | 6.145 | 7.648 |
CC(1/2) | 0.992 | 0.998 | 0.464 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | 2.4 M (NH4)2 SO4, 0.1M MES. pH 6.0 |