6TLA
CRYSTAL STRUCTURE OF LECTIN-LIKE OX-LDL RECEPTOR 1 (C 1 2 1)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2009-12-03 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.91010 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 76.830, 52.190, 109.820 |
| Unit cell angles | 90.00, 92.04, 90.00 |
Refinement procedure
| Resolution | 55.000 - 2.160 |
| R-factor | 0.2116 |
| Rwork | 0.210 |
| R-free | 0.23310 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1ypu |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.910 |
| Data reduction software | autoPROC |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | BUSTER (2.11.7 (3-OCT-2019)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 109.750 | 2.270 |
| High resolution limit [Å] | 2.160 | 2.160 |
| Rmerge | 0.029 | 0.446 |
| Rmeas | 0.035 | 0.552 |
| Rpim | 0.035 | 0.320 |
| Number of reflections | 22997 | 3126 |
| <I/σ(I)> | 19.2 | 2 |
| Completeness [%] | 97.0 | 90.5 |
| Redundancy | 3.1 | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1 M MES pH 6, 20% PEG6000, 0.2 M LiCl |
