6TLA
CRYSTAL STRUCTURE OF LECTIN-LIKE OX-LDL RECEPTOR 1 (C 1 2 1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2009-12-03 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.91010 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 76.830, 52.190, 109.820 |
Unit cell angles | 90.00, 92.04, 90.00 |
Refinement procedure
Resolution | 55.000 - 2.160 |
R-factor | 0.2116 |
Rwork | 0.210 |
R-free | 0.23310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ypu |
RMSD bond length | 0.008 |
RMSD bond angle | 0.910 |
Data reduction software | autoPROC |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | BUSTER (2.11.7 (3-OCT-2019)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 109.750 | 2.270 |
High resolution limit [Å] | 2.160 | 2.160 |
Rmerge | 0.029 | 0.446 |
Rmeas | 0.035 | 0.552 |
Rpim | 0.035 | 0.320 |
Number of reflections | 22997 | 3126 |
<I/σ(I)> | 19.2 | 2 |
Completeness [%] | 97.0 | 90.5 |
Redundancy | 3.1 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1 M MES pH 6, 20% PEG6000, 0.2 M LiCl |