Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-06-01 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.916 |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 103.695, 103.695, 78.769 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 51.847 - 1.530 |
| Rwork | 0.193 |
| R-free | 0.20580 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1axd |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.818 |
| Data reduction software | DIALS |
| Data scaling software | DIALS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 52.000 | 1.600 |
| High resolution limit [Å] | 1.530 | 1.530 |
| Rmerge | 0.034 | 0.079 |
| Rpim | 0.014 | |
| Number of reflections | 38156 | 1848 |
| <I/σ(I)> | 27.3 | |
| Completeness [%] | 100.0 | |
| Redundancy | 12.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | sodium citrate pH 5.6, Na/K tartrate 1.5-2.0 M ammonium sulfate |
