6THJ
CBDP35 Native structure
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-12-07 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.99988 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 332.510, 94.590, 83.190 |
| Unit cell angles | 90.00, 90.40, 90.00 |
Refinement procedure
| Resolution | 37.880 - 2.200 |
| R-factor | 0.1983 |
| Rwork | 0.196 |
| R-free | 0.23840 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6s3y |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.602 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 37.880 | 2.279 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Rmerge | 0.186 | 0.996 |
| Number of reflections | 130198 | 6370 |
| <I/σ(I)> | 6.8 | 1.9 |
| Completeness [%] | 99.6 | 99.2 |
| Redundancy | 6.3 | 6.6 |
| CC(1/2) | 0.993 | 0.686 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 298.5 | 4M Sodium Formate |
