6TF4

Solution structure of RfaH C-terminal domain from Vibrio cholerae

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE		600
2	Bruker	AVANCE		700
3	Bruker	Ascend Aeon		900

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	2	2	3D HBHA(CO)NH
11	2	2	3D CACO
12	2	2	3D CON
13	2	2	3D 1H-13C NOESY aliphatic
14	2	2	3D 1H-13C NOESY aromatic
15	2	2	3D 1H-15N NOESY
16	1	1	3D C(CO)NH
17	2	2	3D long range HNCO
18	2	2	13CO spinecho difference 13C ctHSQC
19	2	2	15N spinecho difference 13C ctHSQC
2	2	2	2D 1H-13C ctHSQC aliphatic
3	2	2	2D 1H-13C HSQC aromatic
4	2	2	3D HNCO
5	2	2	3D HNCA
6	1	1	3D HNCACB
7	1	1	3D CBCA(CO)NH
8	2	2	3D CCH-TOCSY
9	2	2	3D HCCH-TOCSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.5	1	298
2	7.5	1	298

Conformers

Conformers Calculated Total Number	80
Conformers Submitted Total Number	20