6T6Q
Crystal structure of Toxoplasma gondii Morn1 (extended conformation).
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-03-03 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.967 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 53.916, 53.916, 348.849 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.920 - 2.902 |
Rwork | 0.276 |
R-free | 0.31110 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6t4d |
RMSD bond length | 0.002 |
RMSD bond angle | 1.213 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.920 | 3.080 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.140 | 2.252 |
Number of reflections | 12331 | 1819 |
<I/σ(I)> | 11.8 | 0.5 |
Completeness [%] | 99.1 | |
Redundancy | 8.4 | 8 |
CC(1/2) | 0.992 | 0.772 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295.15 | 0.1 M Tris-HCl pH 8.2, 15% PEG 3350, 0.2 M NaCl |