6T5E
Hydroxylamine Oxidoreductase from Brocadia fulgida
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-01 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.00000 |
Spacegroup name | P 21 3 |
Unit cell lengths | 124.560, 124.560, 124.560 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.080 - 3.300 |
R-factor | 0.2224 |
Rwork | 0.220 |
R-free | 0.26420 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4n4j |
RMSD bond length | 0.003 |
RMSD bond angle | 0.886 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 88.080 | 3.400 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmerge | 0.175 | 1.560 |
Rmeas | 0.184 | |
Number of reflections | 18802 | 1404 |
<I/σ(I)> | 11.3 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 10.3 | 10.8 |
CC(1/2) | 0.998 | 0.653 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 1.0 M Lithium chloride, 0.1 M Tris pH 8.5 10% w/v PEG 6K, final pH 8.0 |