6T2Q
Prominent members of the human gut microbiota express endo-acting O-glycanases to initiate mucin breakdown
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 41 |
Unit cell lengths | 82.918, 82.918, 121.310 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.990 - 2.000 |
Rwork | 0.187 |
R-free | 0.21080 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3iln |
RMSD bond length | 0.010 |
RMSD bond angle | 1.626 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.990 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 55261 | 4092 |
<I/σ(I)> | 14 | 1.2 |
Completeness [%] | 99.2 | |
Redundancy | 7.6 | |
CC(1/2) | 0.999 | 0.472 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 450 mM sodium malonate pH 7.0, 24 % PEG 3350 |