6T1D
Pleurotus Ostreatus Lectin (POL), compelx with melibiose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-22 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.87313 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 109.605, 136.421, 110.022 |
Unit cell angles | 90.00, 112.37, 90.00 |
Refinement procedure
Resolution | 29.948 - 2.200 |
R-factor | 0.2145 |
Rwork | 0.212 |
R-free | 0.26510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6t0q |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 47.670 | 101.744 | 2.407 |
High resolution limit [Å] | 2.090 | 7.172 | 2.093 |
Rmerge | 0.151 | 0.055 | 0.821 |
Rmeas | 0.179 | 0.065 | 0.968 |
Rpim | 0.096 | 0.035 | 0.510 |
Total number of observations | 14495 | 15880 | |
Number of reflections | 88942 | 4447 | 4447 |
<I/σ(I)> | 6.6 | 15.8 | 1.7 |
Completeness [%] | 92.5 | 99 | 65.5 |
Redundancy | 3.4 | 3.3 | 3.6 |
CC(1/2) | 0.989 | 0.996 | 0.467 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 K thiocyanate, 30% PEG 2000 MME |