6T0Q
Pleurotus Ostreatus Lectin (POL), apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-01-30 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97625 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 153.070, 153.070, 145.811 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.771 - 2.050 |
R-factor | 0.1726 |
Rwork | 0.172 |
R-free | 0.18660 |
Structure solution method | MIR |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.21) |
Phasing software | SHARP |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 132.562 | 63.882 | 2.160 |
High resolution limit [Å] | 2.050 | 6.480 | 2.050 |
Rmerge | 0.030 | 0.380 | |
Rmeas | 0.071 | 0.032 | 0.395 |
Rpim | 0.020 | 0.010 | 0.107 |
Total number of observations | 790176 | 24968 | 119417 |
Number of reflections | 63266 | 2243 | 9074 |
<I/σ(I)> | 25.9 | 54.1 | 7.4 |
Completeness [%] | 99.8 | 99.4 | 99.7 |
Redundancy | 12.5 | 11.1 | 13.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | Hepes 0.1 M pH 7.5, 0.8 M K/Na tartrate tetrahydrate |