Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2011-06-16 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.979 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 65.150, 170.480, 241.850 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.572 - 2.796 |
| Rwork | 0.242 |
| R-free | 0.26240 |
| Structure solution method | SAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.409 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.600 | 2.960 |
| High resolution limit [Å] | 2.796 | 2.796 |
| Rmeas | 0.277 | 1.690 |
| Number of reflections | 128339 | 20491 |
| <I/σ(I)> | 5.12 | |
| Completeness [%] | 99.7 | |
| Redundancy | 4.29 | |
| CC(1/2) | 0.989 | 0.620 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | 25% PEG3350, 0.2M Ammonium Acetate, 0.05M Bis-Tris buffer, pH 5.5 |
