6SWP
C-TERMINAL BROMODOMAIN OF HUMAN BRD2 WITH iBET-BD2 (GSK046)
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-04-28 |
Detector | RIGAKU |
Wavelength(s) | 1.54178 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 72.201, 52.390, 32.024 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.320 - 1.604 |
Rwork | 0.154 |
R-free | 0.19320 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond angle | 1.183 |
Data reduction software | XDS |
Data scaling software | Aimless |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.320 | 1.690 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 15434 | 1590 |
<I/σ(I)> | 43.4 | 15.7 |
Completeness [%] | 93.4 | |
Redundancy | 2.8 | |
CC(1/2) | 0.998 | 0.974 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 30% PEG 300, 0.1M MES buffer pH6. |