Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, DESY BEAMLINE P11 |
| Synchrotron site | PETRA III, DESY |
| Beamline | P11 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-12-17 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.03320 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 76.258, 76.258, 151.481 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 68.110 - 1.860 |
| Rwork | 0.221 |
| R-free | 0.25600 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.561 |
| Data reduction software | xia2 |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 68.110 | 1.890 |
| High resolution limit [Å] | 1.860 | 1.860 |
| Rmerge | 0.142 | 0.923 |
| Rmeas | 0.145 | 0.956 |
| Number of reflections | 38415 | 1842 |
| <I/σ(I)> | 14.8 | 2.4 |
| Completeness [%] | 100.0 | 99.6 |
| Redundancy | 24.1 | |
| CC(1/2) | 0.999 | 0.540 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 2.2 M ammonium sulfate, 0.2 M tri-potassium citrate |
