6SO0

NMR solution structure of the family 14 carbohydrate binding module (CBM14) from human chitotriosidase

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE III		800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	2	3	2D 1H-1H COSY
11	2	3	2D 1H-1H NOESY
12	1	2	3D 1H-13C NOESY aliphatic
13	1	2	3D 1H-15N NOESY
14	1	2	3D H(CCO)NH
15	2	3	2D 1H-1H TOCSY
2	1	1	3D 1H-15N TOCSY
3	1	2	2D 1H-13C HSQC aliphatic
4	1	2	3D HNCA
5	1	2	3D HNCO
6	1	2	3D CBCA(CO)NH
7	1	2	3D HNCACB
8	1	2	3D HCCH-TOCSY
9	1	2	3D HN(CO)CA

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	5.5	1	298.1
2	5.5	1	298.1

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	20