6SM4
AntF (apo): type II PKS acyl-carrier protein
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-20 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 58.700, 58.700, 149.990 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 1.850 |
R-factor | 0.1584 |
Rwork | 0.158 |
R-free | 0.19610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2fad |
RMSD bond length | 0.006 |
RMSD bond angle | 1.042 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.950 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.043 | 0.556 |
Number of reflections | 23127 | 3301 |
<I/σ(I)> | 24.5 | 3.6 |
Completeness [%] | 99.2 | 99.2 |
Redundancy | 7.2 | |
CC(1/2) | 1.000 | 0.923 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M citric acid, 1 M LiCl, 30% PEG 6000 |