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6SIJ

SAD structure of Hen Egg White Lysozyme recovered by continuous rotation data collection and multivariate analysis of Friedel pairs

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID30B
Synchrotron siteESRF
BeamlineID30B
Temperature [K]100
Detector technologyPIXEL
Collection date2016-07-27
DetectorDECTRIS PILATUS 6M-F
Wavelength(s)1.54980
Spacegroup nameP 43 21 2
Unit cell lengths79.070, 79.070, 36.980
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution39.535 - 1.610
R-factor0.141874113995
Rwork0.141
R-free0.16733
Structure solution methodSAD
RMSD bond length0.006
RMSD bond angle0.819
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareAutoSol
Refinement softwarePHENIX (1.11.1_2575)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]39.5351.650
High resolution limit [Å]1.6101.610
Rmerge0.0790.223
Number of reflections287712102
<I/σ(I)>47.538.84
Completeness [%]99.999.2
Redundancy39.25.8
CC(1/2)1.0000.985
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4.5293.1550mM Na acetate pH 4.5 1M NaCl 25% Ethylene glycol

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