6SHO
SAD structure of Human Survivin recovered by continuous rotation data collection and multivariate analysis of Friedel pairs
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-27 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.27265 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 113.980, 71.020, 81.340 |
Unit cell angles | 90.00, 128.47, 90.00 |
Refinement procedure
Resolution | 35.591 - 3.200 |
R-factor | 0.203720243151 |
Rwork | 0.201 |
R-free | 0.25920 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.183 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | AutoSol |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.600 | 3.280 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.122 | 0.795 |
Number of reflections | 16783 | 1248 |
<I/σ(I)> | 12.04 | 2.03 |
Completeness [%] | 99.1 | 99.1 |
Redundancy | 6.7 | 6.7 |
CC(1/2) | 0.996 | 0.787 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293.15 | 0.2 M NaCitrate pH 6.5, 0.1 M BisTris Propane and 20% PEG3500 |