6SDX
Salmonella ATPase InvC with ATP gamma S
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-07-09 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0332 |
Spacegroup name | P 65 |
Unit cell lengths | 107.898, 107.898, 73.847 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 53.949 - 2.645 |
R-factor | 0.1881 |
Rwork | 0.186 |
R-free | 0.22360 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5swj |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 2.710 |
High resolution limit [Å] | 2.645 | 2.645 |
Rmerge | 0.100 | 1.596 |
Rmeas | 0.106 | 1.694 |
Number of reflections | 14402 | 1041 |
<I/σ(I)> | 16.58 | |
Completeness [%] | 99.8 | |
Redundancy | 10 | |
CC(1/2) | 1.000 | 0.540 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 292.15 | 3M sodium chloride pH 7.5 and 0.1 M Tris |