6SC4
Gamma-Carbonic Anhydrase from the Haloarchaeon Halobacterium sp.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-16 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.28 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 362.640, 362.640, 362.640 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.600 |
R-factor | 0.1787 |
Rwork | 0.177 |
R-free | 0.20440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1v3w |
RMSD bond length | 0.006 |
RMSD bond angle | 1.249 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.700 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.085 | 0.575 |
Number of reflections | 62896 | 12673 |
<I/σ(I)> | 18.8 | 3.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.05 M CdSO4, 0.8 M NaOAc |