6SBC
Structure of type II terpene cyclase MstE from Scytonema in complex with farnesyl dihydroxybenzoate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-08-26 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 47.980, 77.420, 90.910 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 1.350 |
R-factor | 0.1173 |
Rwork | 0.115 |
R-free | 0.15310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6sbb |
RMSD bond length | 0.014 |
RMSD bond angle | 1.852 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.450 |
High resolution limit [Å] | 1.350 | 1.350 |
Rmerge | 0.041 | |
Number of reflections | 72004 | 14057 |
<I/σ(I)> | 15.7 | 2.6 |
Completeness [%] | 95.9 | |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 100 mM HEPES, 4 M NaCl |