6S9P
Designed Armadillo Repeat protein internal Lock2 fused to target peptide KRKAKITWKR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-01-30 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.000031 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 140.680, 37.410, 127.320 |
Unit cell angles | 90.00, 96.59, 90.00 |
Refinement procedure
Resolution | 44.421 - 2.800 |
R-factor | 0.221 |
Rwork | 0.218 |
R-free | 0.26890 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 44.430 | 44.421 | 2.870 |
High resolution limit [Å] | 2.800 | 12.520 | 2.800 |
Rmerge | 0.300 | 0.041 | 1.815 |
Rmeas | 0.325 | 0.045 | 1.987 |
Number of reflections | 16545 | 208 | 1166 |
<I/σ(I)> | 7.12 | 30.56 | 1.27 |
Completeness [%] | 98.6 | 96.3 | 94.8 |
Redundancy | 6.662 | 5.692 | 5.918 |
CC(1/2) | 0.991 | 0.998 | 0.556 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277.15 | 22.5 % PEG smear medium 0.1 M CaCl2, 0.1 M MgCl2, 0.1 M Pipes pH 7 |