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6S82

Structure Of D80A-Fructofuranosidase From Xanthophyllomyces Dendrorhous Complexed With Tris-buffer molecule And hydroquinone

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALBA BEAMLINE XALOC
Synchrotron siteALBA
BeamlineXALOC
Temperature [K]100
Detector technologyPIXEL
Collection date2016-02-12
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.979490
Spacegroup nameP 21 21 2
Unit cell lengths74.579, 205.623, 145.369
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution83.940 - 1.850
R-factor0.1552
Rwork0.154
R-free0.17530
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)5ann
RMSD bond length0.012
RMSD bond angle1.755
Data reduction softwareXDS
Data scaling softwareAimless
Refinement softwareREFMAC (5.8.0238)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]83.9401.880
High resolution limit [Å]1.8501.850
Rmerge0.0790.559
Rpim0.0320.227
Number of reflections19074164488
<I/σ(I)>14.52.9
Completeness [%]100.0
Redundancy6.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2911.3 M Sodium Citrate tribasic dihydrate, 0.1M TRIS-HCl pH 8.5, then soaked in hidroquinone

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