6S7Y
dARC1 capsid domain dimer, hexagonal form at 2.3 Angstrom
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-06-13 |
| Detector | DECTRIS PILATUS 2M-F |
| Wavelength(s) | 0.97941 |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 62.191, 62.191, 400.999 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 53.859 - 2.300 |
| R-factor | 0.249 |
| Rwork | 0.247 |
| R-free | 0.28490 |
| Structure solution method | SAD |
| Data reduction software | xia2 (0.5.546-gdf2e053-dials-1.9) |
| Data scaling software | pointless (1.11.12) |
| Phasing software | AutoSol (1.14_3260) |
| Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 57.290 | 2.200 |
| High resolution limit [Å] | 2.140 | 2.140 |
| Rmerge | 0.119 | 0.983 |
| Rmeas | 0.122 | 1.029 |
| Rpim | 0.025 | 0.298 |
| Number of reflections | 26972 | 1886 |
| <I/σ(I)> | 22 | 2.6 |
| Completeness [%] | 99.9 | 99.3 |
| Redundancy | 40.8 | 22.4 |
| CC(1/2) | 1.000 | 0.517 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298 | NaCl 2.8-3.3 M, 0.1 M HEPES pH 7.5 |
