6S7X

dARC1 capsid domain dimer, orthorhombic form at 1.7 Angstrom

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-06-13
Detector	DECTRIS PILATUS 2M-F
Wavelength(s)	0.98399
Spacegroup name	P 21 21 21
Unit cell lengths	62.334, 70.386, 142.821
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	71.410 - 1.700
R-factor	0.1824
Rwork	0.181
R-free	0.21280
Structure solution method	SAD
RMSD bond length	0.010
RMSD bond angle	1.707
Data reduction software	XDS (Jan 26, 2018 (BUILT 20180409))
Data scaling software	AutoPROC (1.0.5)
Phasing software	AutoSol (1.14_3260)
Refinement software	REFMAC (5.8.0238)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	71.410	1.700
High resolution limit [Å]	1.550	1.550
Rmeas	0.093	1.501
Rpim	0.029	0.478
Number of reflections	48232	2412
<I/σ(I)>	10.3	1.5
Completeness [%]	84.1	66
Redundancy	10	9.7
CC(1/2)	0.998	0.557

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.5	298	NaCl 2.8-3.3 M, 0.1 M HEPES pH 7.5