6S4M
Crystal structure of the human organic anion transporter MFSD10 (TETRAN)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-06 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9687 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.994, 70.375, 63.440 |
Unit cell angles | 90.00, 115.45, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.400 |
R-factor | 0.2112 |
Rwork | 0.209 |
R-free | 0.25830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3wdo |
RMSD bond length | 0.007 |
RMSD bond angle | 1.458 |
Data reduction software | XDS (20190315) |
Data scaling software | Aimless (0.7.4) |
Phasing software | PHASER (2.8.2) |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.740 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.208 | 1.657 |
Rmeas | 0.234 | 1.853 |
Rpim | 0.104 | 0.822 |
Number of reflections | 17297 | 1822 |
<I/σ(I)> | 5.7 | 1 |
Completeness [%] | 98.7 | 98.2 |
Redundancy | 4.9 | 5 |
CC(1/2) | 0.990 | 0.399 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 6.5 | 293 | 0.1M ADA pH6.5 -- 0.2M lithium citrate -- 30% PEG400 |