6S2Y
Water-soluble Chlorophyll Protein (WSCP) from Lepidium virginicum with Chlorophyll-b
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR-H |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2018-07-04 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.310, 82.900, 122.220 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.630 - 2.300 |
R-factor | 0.2451 |
Rwork | 0.243 |
R-free | 0.27660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2dre |
RMSD bond length | 0.010 |
RMSD bond angle | 2.384 |
Data reduction software | XDS (VERSION Mar 15, 2019) |
Data scaling software | XSCALE (VERSION Mar 15, 2019) |
Phasing software | PHASER (2.8.2) |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.630 | 2.360 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.078 | |
Number of reflections | 33323 | 2427 |
<I/σ(I)> | 12.31 | 3.03 |
Completeness [%] | 98.7 | 99.8 |
Redundancy | 4.62 | 4.76 |
CC(1/2) | 0.997 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 0.1M Na/K Phosphate, 3.0M Ammonium sulfate, 4.7% Sucrose |