6S10

NMR solution structure of a ProQ homolog from Legionella pneumophila

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE		600
2	Bruker	AVANCE		700
3	Bruker	AVANCE		800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	1	3D 1H-15N NOESY
11	1	2	3D 1H-13C NOESY aliphatic
12	1	2	3D 1H-13C NOESY aromatic
13	1	2	2D 1H-13C HSQC aliphatic
14	1	3	2D 1H-15N HSQC
15	1	4	2D 1H-15N HSQC
16	1	5	2D 1H-15N HSQC
17	1	5	2D 1H-13C HSQC aliphatic
18	1	6	3D 1H-13C NOESY aliphatic
2	1	2	2D 1H-13C HSQC aromatic
3	1	2	3D HNCO
4	1	2	3D HCACO
5	1	2	3D HNCACB
6	1	2	3D HBHA(CO)NH
7	1	2	3D HCCH-TOCSY
8	1	2	3D H(CCO)NH
9	1	2	3D C(CO)NH

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.5	AMBIENT	298

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	20