6RYX
Copper oxidase from Colletotrichum graminicola
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-09-21 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.91587 |
Spacegroup name | I 2 3 |
Unit cell lengths | 172.043, 172.043, 172.043 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 121.650 - 2.650 |
R-factor | 0.2241 |
Rwork | 0.221 |
R-free | 0.27970 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5c86 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.668 |
Data reduction software | DIALS |
Data scaling software | Aimless |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 121.650 | 2.780 |
High resolution limit [Å] | 2.650 | 2.650 |
Rmerge | 0.215 | |
Rpim | 0.045 | 0.581 |
Number of reflections | 24743 | 3283 |
<I/σ(I)> | 12 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 24.2 | 23.3 |
CC(1/2) | 0.998 | 0.535 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 291 | PEG 4000, sodium acetate |