6RYL
WUS-HD bound to TAAT DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-18 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97242 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 82.663, 45.914, 87.535 |
Unit cell angles | 90.00, 102.88, 90.00 |
Refinement procedure
Resolution | 41.752 - 2.630 |
R-factor | 0.2385 |
Rwork | 0.237 |
R-free | 0.26360 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ry3 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.736 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.920 | 2.724 |
High resolution limit [Å] | 2.630 | 2.630 |
Rpim | 0.038 | |
Number of reflections | 19403 | 1907 |
<I/σ(I)> | 11.6 | |
Completeness [%] | 99.4 | |
Redundancy | 4.5 | |
CC(1/2) | 0.552 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1 M CHES (pH 9.5), 20% PEG 8000 |