6RYI
WUS-HD bound to G-Box DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-3 |
Synchrotron site | ESRF |
Beamline | MASSIF-3 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-08 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 0.96769 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 123.434, 83.068, 85.651 |
Unit cell angles | 90.00, 112.95, 90.00 |
Refinement procedure
Resolution | 40.667 - 2.691 |
R-factor | 0.1971 |
Rwork | 0.194 |
R-free | 0.25110 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ry3 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.105 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.670 | 2.788 |
High resolution limit [Å] | 2.690 | 2.691 |
Rpim | 0.052 | |
Number of reflections | 21967 | 2053 |
<I/σ(I)> | 10.97 | |
Completeness [%] | 98.1 | |
Redundancy | 4.8 | |
CC(1/2) | 0.458 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2 M lithium acetate, 20% PEG 3350 |