6RY5
Crystal structure of Dfg5 from Chaetomium thermophilum in complex with alpha-1,6-mannobiose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.072 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 83.415, 55.019, 80.119 |
Unit cell angles | 90.00, 90.37, 90.00 |
Refinement procedure
Resolution | 45.928 - 1.300 |
R-factor | 0.1027 |
Rwork | 0.102 |
R-free | 0.12330 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.599 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.930 | 1.346 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.020 | 0.094 |
Rmeas | 0.028 | |
Number of reflections | 85994 | 8464 |
<I/σ(I)> | 20.02 | 6.93 |
Completeness [%] | 96.4 | 95.07 |
Redundancy | 1.9 | 1.8 |
CC(1/2) | 0.999 | 0.975 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 291.15 | Ammoniumiodide, PEG3350, Calcium acetate, MES, PEG 8000 |