6RVQ
SaFtsz-GDP-EthGLy
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-03-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 72.373, 50.500, 88.431 |
Unit cell angles | 90.00, 111.52, 90.00 |
Refinement procedure
Resolution | 33.464 - 1.136 |
R-factor | 0.2078 |
Rwork | 0.207 |
R-free | 0.21400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6rvn |
RMSD bond length | 0.008 |
RMSD bond angle | 1.113 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.200 |
High resolution limit [Å] | 1.136 | 1.140 |
Number of reflections | 108093 | 15595 |
<I/σ(I)> | 11.5 | |
Completeness [%] | 99.1 | |
Redundancy | 3.3 | |
CC(1/2) | 0.998 | 0.716 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 27.5 % PEG 5K MME, 10 % EthGly, 0.2 M Li2SO4, 0.1 M Tris pH 9.0 |