6RVP
SaFtsz-GDP-MetPyr
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9790 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 72.477, 50.079, 88.502 |
Unit cell angles | 90.00, 111.78, 90.00 |
Refinement procedure
Resolution | 36.207 - 1.160 |
R-factor | 0.1916 |
Rwork | 0.191 |
R-free | 0.20830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6rvn |
RMSD bond length | 0.009 |
RMSD bond angle | 1.115 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.220 |
High resolution limit [Å] | 1.160 | 1.160 |
Number of reflections | 92535 | 8143 |
<I/σ(I)> | 13.4 | |
Completeness [%] | 91.0 | |
Redundancy | 13.4 | |
CC(1/2) | 0.999 | 0.635 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 26% PEG 5K MME, 10% EthGly, 0.2 M LI2SO4, 0.1 M Tris pH 8.7 |