6RTA
Tetragonal lysozyme grown with 300g/L Ficoll
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | OXFORD DIFFRACTION GEMINI |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-12-20 |
Detector | OXFORD ONYX CCD |
Wavelength(s) | 1.54056 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.662, 78.662, 37.105 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 14.607 - 1.800 |
R-factor | 0.1657 |
Rwork | 0.164 |
R-free | 0.19120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2w1x |
RMSD bond length | 0.006 |
RMSD bond angle | 0.792 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.15.2_3472: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 14.610 | 1.840 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.083 | 0.720 |
Rmeas | 0.093 | 0.890 |
Rpim | 0.042 | 0.510 |
Number of reflections | 11092 | 616 |
<I/σ(I)> | 15.5 | 1.3 |
Completeness [%] | 98.5 | 95.5 |
Redundancy | 4.7 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.7 | 310 | 0.2M Sodium Acetate pH 4.7, 3% (w/v) NaCl, 300 g/L Ficoll |