6RT9
Orthorhombic lysozyme grown with 300g/L sucrose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | OXFORD DIFFRACTION GEMINI |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-12-19 |
Detector | OXFORD ONYX CCD |
Wavelength(s) | 1.54056 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 30.065, 56.091, 72.455 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 14.785 - 1.550 |
R-factor | 0.1863 |
Rwork | 0.184 |
R-free | 0.22780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2w1x |
RMSD bond length | 0.005 |
RMSD bond angle | 0.887 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.15.2_3472: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 14.785 | 1.580 |
High resolution limit [Å] | 1.550 | 1.550 |
Rmerge | 0.071 | 0.872 |
Rmeas | 0.085 | |
Rpim | 0.044 | 0.754 |
Number of reflections | 18289 | 859 |
<I/σ(I)> | 11.7 | 0.8 |
Completeness [%] | 99.1 | 95.5 |
Redundancy | 3.3 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.7 | 310 | 0.2M Sodium Acetate pH 4.7, 3% (w/v) NaCl, 300 g/L sucrose |