6RT1
Native tetragonal lysozyme - home source data
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | OXFORD DIFFRACTION GEMINI |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-06-24 |
Detector | OXFORD ONYX CCD |
Wavelength(s) | 1.54056 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.634, 78.634, 36.993 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 14.602 - 1.336 |
R-factor | 0.1241 |
Rwork | 0.122 |
R-free | 0.16180 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2w1x |
RMSD bond length | 0.006 |
RMSD bond angle | 0.907 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.15.2_3472: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 14.602 | 1.360 |
High resolution limit [Å] | 1.336 | 1.340 |
Rmerge | 0.068 | |
Rmeas | 0.069 | |
Rpim | 0.014 | |
Number of reflections | 26070 | 655 |
<I/σ(I)> | 30.4 | |
Completeness [%] | 96.9 | 50.7 |
Redundancy | 20.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.8 | 293 | 100 mM Sodium Acetate pH 4.8, 10% (w/v) NaCl, 25% (v/v) Ethylene Glycol |