6RR9

DNA/RNA binding protein

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-03-04
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	1.28
Spacegroup name	P 32 2 1
Unit cell lengths	101.060, 101.060, 114.460
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.777 - 3.432
R-factor	0.2104
Rwork	0.205
R-free	0.25880
Structure solution method	SAD
RMSD bond length	0.013
RMSD bond angle	1.414
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX ((1.15.2_3472: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.780	3.630
High resolution limit [Å]	3.400	3.400
Number of reflections	17172	2557
<I/σ(I)>	12.2
Completeness [%]	98.0
Redundancy	8.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.1 M sodium acetate pH5.0, 1.5M ammonium sulfate