6RQP
Steady-state-SMX dark state structure of bacteriorhodopsin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 298 |
Detector technology | PIXEL |
Collection date | 2018-05-06 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 63 |
Unit cell lengths | 62.000, 62.000, 110.300 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.336 - 1.800 |
R-factor | 0.1753 |
Rwork | 0.174 |
R-free | 0.19840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6g7h |
Data reduction software | CrystFEL (0.7) |
Data scaling software | CrystFEL (0.7) |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.800 | 1.850 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 22272 | |
<I/σ(I)> | 14.3 | 1.17 |
Completeness [%] | 100.0 | 100 |
Redundancy | 1587.9 | 198.2 |
CC(1/2) | 0.990 | 0.310 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 5.6 | 294 | 100 mM Na/K Phosphate buffer pH 5.6 30 % PEG 2000 |