6RPQ
Crystal structure of PhoCDC21-1 intein
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-14 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9159 |
Spacegroup name | I 41 |
Unit cell lengths | 100.920, 100.920, 91.720 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.460 | 3.010 | 2.810 |
High resolution limit [Å] | 2.650 | 2.810 | 2.650 |
Rmeas | 0.094 | 0.860 | 1.679 |
Number of reflections | 13373 | 2011 | 2154 |
<I/σ(I)> | 18.23 | 2.62 | 1.24 |
Completeness [%] | 100.0 | 100 | 99.9 |
Redundancy | 13.8 | 13.7 | 14.2 |
CC(1/2) | 0.999 | 0.923 | 0.713 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | tri-ammonium citrate |