6RN5
PptA from Streptomyces chartreusis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-08-01 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.905002 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 49.303, 132.233, 116.398 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.196 - 2.037 |
R-factor | 0.193 |
Rwork | 0.191 |
R-free | 0.23700 |
Structure solution method | SAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.532 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0218 2018/15/02) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.196 | 2.160 |
High resolution limit [Å] | 2.037 | 2.037 |
Rmerge | 0.106 | 0.916 |
Rmeas | 0.111 | 0.971 |
Number of reflections | 24547 | 3733 |
<I/σ(I)> | 19.2 | 2.26 |
Completeness [%] | 98.9 | 94.5 |
Redundancy | 12.3 | 8.9 |
CC(1/2) | 0.999 | 0.711 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 295 | 100 mM MES/HCl pH 6.5, 1.6 M MgSO4 |