6RK1
Crystal structure of TSP1 domain from CCN3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-07-02 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.930 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 52.860, 52.860, 102.390 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.130 - 1.630 |
R-factor | 0.1626 |
Rwork | 0.162 |
R-free | 0.18440 |
Structure solution method | MAD |
RMSD bond length | 0.005 |
RMSD bond angle | 0.751 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.130 | 1.660 |
High resolution limit [Å] | 1.630 | 1.630 |
Rmerge | 0.082 | |
Number of reflections | 2082 | 220 |
<I/σ(I)> | 13 | |
Completeness [%] | 100.0 | |
Redundancy | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 293 | 3.0 M NaCl, 0.1 M Tris pH 8.0 |