6RH6
Solution structure and 1H, 13C and 15N chemical shift assignments for the complex of NECAP1 PHear domain with phosphorylated AP2 mu2 148-163
Spectrometer
Experimental method: SOLUTION NMR
Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
1 | Bruker | AVANCE III | 600 | |
2 | Bruker | AVANCE | 600 | |
3 | Bruker | AVANCE III | 800 |
Experiment
experiment id | conditions id | solution id | Experiment type |
10 | 1 | 3 | 2D 1H-13C HSQC aliphatic (constant time) |
11 | 1 | 3 | 2D 1H-13C HSQC aromatic (constant time) |
12 | 1 | 3 | 2D 1H-1H NOESY (reject 15N,13C coupled 1H in F1, accept 13C coupled 1H in F2) tau(m) 150ms |
13 | 1 | 2 | 3D HBHA(CO)NH |
14 | 1 | 2 | 3D HNCACB |
15 | 1 | 3 | 3D HCCH-COSY (1H,13C,1H) |
16 | 1 | 3 | 3D HCCH-TOCSY (13C,13C,1H) |
17 | 1 | 2 | 3D 1H-15N NOESY tau(m) 150ms |
18 | 1 | 2 | 3D 1H-13C NOESY aliphatic tau(m) 150ms |
19 | 1 | 3 | 3D 1H-13C NOESY aliphatic tau(m) 150ms |
2 | 1 | 2 | 2D 1H-15N HSQC |
20 | 1 | 2 | 3D 1H-13C NOESY aromatic tau(m) 150ms |
21 | 1 | 3 | 3D 1H-13C NOESY aromatic tau(m) 150ms |
22 | 1 | 2 | 3D 1H-13C NOESY aliphatic (reject 15N,13C coupled 1H in F1) tau(m) 150ms |
23 | 1 | 3 | 3D 1H-13C NOESY aliphatic (reject 15N,13C coupled 1H in F1) tau(m) 150ms |
24 | 1 | 2 | 3D 1H-13C NOESY aromatic (reject 15N,13C coupled 1H in F1) tau(m) 150ms |
25 | 1 | 3 | 3D 1H-13C NOESY aromatic (reject 15N,13C coupled 1H in F1) tau(m) 150ms |
3 | 1 | 2 | 2D 1H-13C HSQC aliphatic |
4 | 1 | 2 | 2D 1H-13C HSQC aromatic |
5 | 1 | 2 | 2D 1H-1H NOESY (reject 15N,13C coupled 1H in F1, accept 15N,13C coupled 1H in F2) tau(m) 150ms |
6 | 1 | 2 | 2D 1H-1H NOESY (reject 15N,13C coupled 1H in F1 and F2) tau(m) 150ms |
7 | 1 | 2 | 2D 1H-1H TOCSY (reject 15N,13C coupled 1H in F2) |
8 | 1 | 3 | 2D 1H-13C HSQC aliphatic |
9 | 1 | 3 | 2D 1H-13C HSQC aromatic |
NMR Sample
conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
1 | 7 | 1 | 298 |
Conformers
Conformers Calculated Total Number | 50 |
Conformers Submitted Total Number | 30 |