6RH5
Solution structure and 1H, 13C and 15N chemical shift assignments for NECAP1 PHear domain
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE III | 600 | |
| 2 | Bruker | AVANCE | 600 | |
| 3 | Bruker | AVANCE III | 800 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D 1H-15N HSQC |
| 10 | 1 | 1 | 3D HCCH-COSY (1H,13C,1H) |
| 11 | 1 | 1 | 3D HBHA(CO)NH |
| 12 | 1 | 1 | 3D HNCACB |
| 13 | 1 | 1 | 3D CBCA(CO)NH |
| 14 | 1 | 1 | 3D HNCA |
| 2 | 1 | 1 | 2D 1H-13C HSQC aliphatic |
| 3 | 1 | 1 | 2D 1H-13C HSQC aromatic |
| 4 | 1 | 1 | 2D 1H-13C HSQC aliphatic (constant time) |
| 5 | 1 | 1 | 2D 1H-13C HSQC aromatic (constant time) |
| 6 | 1 | 1 | 3D 1H-13C NOESY aromatic tau(m) 150ms |
| 7 | 1 | 1 | 3D 1H-13C NOESY aliphatic tau(m) 150ms |
| 8 | 1 | 1 | 3D 1H-15N NOESY tau(m) 150ms |
| 9 | 1 | 1 | 3D HCCH-TOCSY (13C,13C,1H) |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 7 | 1 | 298 |
Conformers
| Conformers Calculated Total Number | 50 |
| Conformers Submitted Total Number | 30 |
