6RGV
Truncated FljB phase 2 flagellin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-02-03 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.91841 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 97.468, 38.280, 124.690 |
Unit cell angles | 90.00, 103.54, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.000 |
Rwork | 0.213 |
R-free | 0.25850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1io1 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.325 |
Data reduction software | XDS (December 6, 2010) |
Data scaling software | XSCALE (December 6, 2010) |
Phasing software | PHASER (2.5.2) |
Refinement software | CNS (1.3) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.050 |
High resolution limit [Å] | 2.000 | 8.930 | 2.000 |
Rmerge | 0.096 | 0.036 | 0.673 |
Rmeas | 0.106 | 0.040 | 0.752 |
Total number of observations | 169968 | ||
Number of reflections | 30567 | 388 | 1927 |
<I/σ(I)> | 11.25 | 25.66 | 2.26 |
Completeness [%] | 98.7 | 99.5 | 86 |
Redundancy | 5.561 | 5.418 | 4.651 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 289 | 0.1 M Tris (pH 8.5), 20% (w/v) PEG4000, 24% (v/v) isopropanol |