6RGN
BteA131
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-11-27 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.916 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 51.428, 51.428, 82.712 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 36.390 - 2.010 |
| R-factor | 0.17604 |
| Rwork | 0.173 |
| R-free | 0.23226 |
| Structure solution method | SAD |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.939 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SHELXCD |
| Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 43.670 | 2.059 |
| High resolution limit [Å] | 2.010 | 2.010 |
| Number of reflections | 7548 | 390 |
| <I/σ(I)> | 79.26 | |
| Completeness [%] | 100.0 | |
| Redundancy | 25.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Sodium acetate pH 4.5 and 2 M Ammonium sulfate |
