6RC9
P1 Mycoplasma pneumoniae
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 80 |
| Detector technology | PIXEL |
| Collection date | 2018-05-24 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97897 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 132.897, 115.637, 96.341 |
| Unit cell angles | 90.00, 117.67, 90.00 |
Refinement procedure
| Resolution | 72.200 - 1.940 |
| R-factor | 0.189 |
| Rwork | 0.187 |
| R-free | 0.22900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.150 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | BUSTER (2.10.3) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 72.200 | 2.040 |
| High resolution limit [Å] | 1.935 | 1.940 |
| Number of reflections | 92405 | |
| <I/σ(I)> | 6.9 | |
| Completeness [%] | 96.5 | |
| Redundancy | 3.5 | |
| CC(1/2) | 0.993 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4 | 293.15 | PEGMME2000 and PCB buffer |
