6RA7
Human tnik in complex with compound 9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-21 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.976 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.916, 53.667, 127.927 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 128.000 - 1.200 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | AMoRE |
Refinement software | BUSTER-TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 128.000 | 1.300 |
High resolution limit [Å] | 1.200 | 1.200 |
Number of reflections | 400672 | 955 |
<I/σ(I)> | 13.3 | |
Completeness [%] | 72.4 | |
Redundancy | 2.4 | |
CC(1/2) | 0.993 | 0.512 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 25% PEG3350 w/v, 0.1M PCTP (pH 8.0), 200 mM sodium formate w/v |