6R9I
Structure of Saccharomyces cerevisiae apo Pan2 pseudoubiquitin hydrolase-RNA exonuclease (UCH-Exo) module
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-10-14 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 91.373, 117.075, 255.319 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 86.030 - 3.000 |
R-factor | 0.2456 |
Rwork | 0.243 |
R-free | 0.28950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4czw |
Data reduction software | XDS |
Data scaling software | xia2 (1.12) |
Phasing software | PHASER (2.8) |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 106.410 | 3.080 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.093 | 1.761 |
Number of reflections | 27902 | 1350 |
<I/σ(I)> | 12.4 | 1.3 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 6.6 | 6.6 |
CC(1/2) | 0.998 | 0.774 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.4 M ammonium phosphate |