6R80
Structure of AFF4 C-terminal homology domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-30 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97925 |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 41.530, 79.480, 185.440 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.360 - 2.200 |
R-factor | 0.2334 |
Rwork | 0.232 |
R-free | 0.25150 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 0.460 |
Data reduction software | XDS (VERSION Nov 11, 2017) |
Data scaling software | XSCALE (VERSION Jan 26, 2018) |
Phasing software | HKL2Map (Version 0.4.e-beta) |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.260 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 16107 | 2204 |
<I/σ(I)> | 11.04 | 1.11 |
Completeness [%] | 100.0 | 100 |
Redundancy | 6.97 | 6.85 |
CC(1/2) | 0.999 | 0.663 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 291.15 | PEG 8000 14%-16% KH2PO4 0.04 M Glycerol 20% |